I need help with the two molecular structures from each attachment below! Thank you in advance!
Callam/Paul Chemistry 2550 Autumn 2016 Spectroscopy Unknown Pre-Lecture Quiz 7 5 points ? Thursday Lecture (11/17/2016) Spectroscopy Unknown. The spectra and data provided were obtained from a pure organic molecule. 1
For H NMR Spectra, the integral is given in number of hydrogens (#H) or as a relative ratio. Important coupling constants (J-values) are listed next to the peaks for some examples. For some spectra, an inset (grey box) is also given showing a ?zoom-in? on an important part of the spectrum. Submit your answer for Quiz 7 at: www.go.osu.edu/2550Quiz Mass Spectrum (not shown): [M] = 264 (51%), 266 (100%), 268 (49%) m/z -1
IR Spectrum (not shown): 3060, 2985, 1600, 1495 cm (all listed are strong (s) unless otherwise indicated) 1
H NMR Spectrum (400 MHz, CDCl3, 25 ?C) s d (J = 8 Hz) t (J = 8 Hz) 8 7
2H 6 5 4
PPM 1H 3 2 1 0 3H 13 C NMR Spectrum (with DEPT), proton-decoupled (125 MHz, CDCl3, 25 ?C) (C) 160 (CH) (CH) 140 (C) 120 (CH 3) 100 PPM 80 60 40 20 0 Q7.R 1/1
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